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Iranian Journal of Materials Science and Engineering، جلد ۱۷، شماره ۲، صفحات ۰-۰
عنوان فارسی
چکیده فارسی مقاله
کلیدواژه‌های فارسی مقاله
عنوان انگلیسی Effect of Heat Treatment on Formation of Calcium Titanate Hollow-Crystals Nanostructures Prepared by Hydrothermal Method
چکیده انگلیسی مقاله In this research, calcium titanate (CaTiO3) hollow crystals have been successfully prepared via hydrothermal method. Titanium tetrachloride, calcium chloride dihydrate and potassium hydroxide were used as Ti, Ca and precipitating agent, respectively. The hydrothermal synthesis was performed at different temperatures and time durations. The negative amount of the Gibbs free energy shows the reactivity of the reaction at room temperature. Characterization of CaTiO3 was carried out using scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD). The optimum condition for preparing CaTiO3 is the sample kept in an autoclave at 300 ℃ for 3 h that requires less energy and time which consists of a high degree of crystallinity. In this research, tetragonal CaTiO3 hollow crystals have been successfully prepared via hydrothermal method. TiCl4, CaCl2.2H2O, and KOH were used as Ti, Ca and precipitating agent, respectively. The hydrothermal synthesis was performed at different temperatures and time durations. Characterization of CaTiO3 was carried out using SEM, HRTEM, and XRD. The sample kept in the autoclave at 300 ℃ for 3 h well crystallized and required less energy and time for synthesis. The powder has a homogenous dispersity of crystals with the range of nanometer to micrometer sizes which makes it a good candidate as a photocatalyst material
کلیدواژه‌های انگلیسی مقاله hydrothermal, crystal growth, morphology, nanostructure
نویسندگان مقاله | S. Manafi
Department of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Iran


| S. Joughehdoust
Department of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Iran
نشانی اینترنتی http://ijmse.iust.ac.ir/browse.php?a_code=A-10-2144-1&slc_lang=en&sid=1
فایل مقاله اشکال در دسترسی به فایل - ./files/site1/rds_journals/454/article-454-2411316.pdf
کد مقاله (doi)
زبان مقاله منتشر شده en
موضوعات مقاله منتشر شده گروه سرامیک
نوع مقاله منتشر شده Research paper
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