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Iranian Journal of Chemistry and Chemical Engineering، جلد ۴۱، شماره ۸، صفحات ۲۶۳۵-۲۶۴۹
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عنوان انگلیسی Synthesis, Characterization, X-Ray Diffraction Analysis of A Tridentate Schiff Base Ligand and Its Complexes with Co(II), Fe(II), Pd(II) and Ru(II): Bioactivity Studies
چکیده انگلیسی مقاله This study reports the synthesis of Co(II), Fe(II), Pd(II), and Ru(II) complexes with Schiff base obtained by the condensation of 2-amino-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate with salicylaldehyde. The characterization of the ligand and its complexes was arranged and studied by FT-IR, UV-Vis., 1H and 13C NMR, microanalyses (C, H, N, S), X-Ray Diffraction (XRD) analysis, magnetic susceptibility, mass spectra, and ThermoGravimetry Analysis (TGA) and further was screened for antimicrobial, antioxidant and antiradical activities. The antioxidant activity of the ligand and its metal complexes was examined by using different methods including the total antioxidant activity method, total reduction method, and DPPH. The antimicrobial activities of Schiff base and metal complexes were investigated on bacterial and fungal strains. DNA cleavage experiments of metal complexes with supercoiled pBR322 DNA were detected by gel electrophoresis in the being of H2O2.
کلیدواژه‌های انگلیسی مقاله DNA cleavage,Antimicrobial,Antioxidant,X-ray diffraction analysis,Schiff Base,Metal Complexes
نویسندگان مقاله Kenan Buldurun |
Department of Food Processing, Vocational School of Technical Sciences, Muş Alparslan University, 49250 Muş, TURKEY

Nevin Turan |
Department of Chemistry, Faculty of Arts and Sciences, Muş Alparslan University, 49250 Muş, TURKEY

Ahmet Savcı |
Department of Molecular Biology and Genetics, Faculty of Arts and Sciences, Muş Alparslan University, 49250 Muş, TURKEY

Yusuf Alan |
Department of Molecular Biology and Genetics, Faculty of Arts and Sciences, Muş Alparslan University, 49250 Muş, TURKEY

Naki Colak |
Department of Chemistry, Faculty of Arts and Sciences, Hitit University, 19100 Çorum, TURKEY

نشانی اینترنتی https://ijcce.ac.ir/article_246858_c90eea5d2b3d5366f2b0bf492518f5ce.pdf
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